C₇H₆I₂O

Base Information

• Chemical Name: C₇H₆I₂O
• CAS No.: 1418218-67-3
• Molecular Formula: C₇H₆I₂O
• Molecular Weight: 359.933
• Mol file: 1418218-67-3.mol

Synonyms:

Chemical Property of C₇H₆I₂O

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₇H₆I₂O

There total 3 articles about C₇H₆I₂O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

3,4-diiodobenzoic acid (35674-20-5) → C7H6I2O (1418218-67-3)

Guidance literature:

With dimethyl sulfide borane; In tetrahydrofuran;

DOI:10.1016/j.tetlet.2012.11.102

Reference yield:

4-amino-benzoic acid (150-13-0,159246-81-8,8014-65-1) → C7H6I2O (1418218-67-3)

Guidance literature:

Multi-step reaction with 3 steps

1: sodium periodate; potassium iodide / water; methanol

2: potassium iodide; sodium nitrite; sulfuric acid

3: dimethyl sulfide borane / tetrahydrofuran

With sodium periodate; sulfuric acid; dimethyl sulfide borane; potassium iodide; sodium nitrite; In tetrahydrofuran; methanol; water;

DOI:10.1016/j.tetlet.2012.11.102

Reference yield:

4-amino-3-iodobenzoic acid (2122-63-6) → C7H6I2O (1418218-67-3)

Guidance literature:

Multi-step reaction with 2 steps

1: potassium iodide; sodium nitrite; sulfuric acid

2: dimethyl sulfide borane / tetrahydrofuran

With sulfuric acid; dimethyl sulfide borane; potassium iodide; sodium nitrite; In tetrahydrofuran;

DOI:10.1016/j.tetlet.2012.11.102

upstream raw materials:

4-amino-benzoic acid

4-amino-3-iodobenzoic acid

3,4-diiodobenzoic acid

Downstream raw materials:

C₂₄H₃₁NO₅

C₈H₈I₂O₃S

Refernces