Technology Process of 2-{[4-(4-hexylbenzoyl)benzoyl]oxy}-N,N,N-trimethylethanaminium bromide
There total 6 articles about 2-{[4-(4-hexylbenzoyl)benzoyl]oxy}-N,N,N-trimethylethanaminium bromide which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
In
acetonitrile;
15 min, cooling; 12 h room temperature;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 80 percent / AlCl3 / 1,2-dichloro-ethane / 36 h
2: 80 percent / H2O, KOH / methanol / 3 h / Heating
3: thionylchloride / 3 h / Heating
4: 65 percent / petroleum ether / 29 h / Ambient temperature
5: 27 percent / acetonitrile / 15 min, cooling; 12 h room temperature
With
potassium hydroxide; aluminium trichloride; thionyl chloride; water;
In
methanol; 1,2-dichloro-ethane; acetonitrile; Petroleum ether;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 80 percent / AlCl3 / 1,2-dichloro-ethane / 36 h
2: 80 percent / H2O, KOH / methanol / 3 h / Heating
3: thionylchloride / 3 h / Heating
4: 65 percent / petroleum ether / 29 h / Ambient temperature
5: 27 percent / acetonitrile / 15 min, cooling; 12 h room temperature
With
potassium hydroxide; aluminium trichloride; thionyl chloride; water;
In
methanol; 1,2-dichloro-ethane; acetonitrile; Petroleum ether;
