Technology Process of C11H13ClN2O
There total 5 articles about C11H13ClN2O which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
sodium tetrahydroborate; cobalt(II) chloride;
In
methanol;
at 100 ℃;
for 0.333333h;
Microwave irradiation;
DOI:10.1016/j.bmcl.2011.02.009
- Guidance literature:
-
Multi-step reaction with 2 steps
1: hydrogenchloride / diethyl ether; water / 4 h / 20 °C
2: sodium tetrahydroborate; cobalt(II) chloride / methanol / 0.33 h / 100 °C / Microwave irradiation
With
hydrogenchloride; sodium tetrahydroborate; cobalt(II) chloride;
In
methanol; diethyl ether; water;
DOI:10.1016/j.bmcl.2011.02.009
- Guidance literature:
-
Multi-step reaction with 3 steps
1: potassium tert-butylate / tert-butyl alcohol / 20 °C
2: hydrogenchloride / diethyl ether; water / 4 h / 20 °C
3: sodium tetrahydroborate; cobalt(II) chloride / methanol / 0.33 h / 100 °C / Microwave irradiation
With
hydrogenchloride; sodium tetrahydroborate; potassium tert-butylate; cobalt(II) chloride;
In
methanol; diethyl ether; water; tert-butyl alcohol;
DOI:10.1016/j.bmcl.2011.02.009