2.3.4-Trichlorbenzamid

Base Information

• Chemical Name: 2.3.4-Trichlorbenzamid
• CAS No.: 24055-86-5
• Molecular Formula: C₇H₄Cl₃NO
• Molecular Weight: 224.474
• Mol file: 24055-86-5.mol

Synonyms:

Chemical Property of 2.3.4-Trichlorbenzamid

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2.3.4-Trichlorbenzamid

There total 3 articles about 2.3.4-Trichlorbenzamid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2,3,4-tri-chloro-benzonitrile (2112-31-4) → 2.3.4-Trichlorbenzamid (24055-86-5)

Guidance literature:

With sulfuric acid; at 70 ℃;

DOI:10.1002/ps.2780410210

Reference yield:

2,3,4-trichloroaniline (634-67-3) → 2.3.4-Trichlorbenzamid (24055-86-5)

Guidance literature:

Multi-step reaction with 2 steps

1.1: NaNO₂; aq. HCl

1.2: copper(I) cyanide / H₂O / 0.33 h / 20 °C

2.1: 70 percent H₂SO₄ / 70 °C

With hydrogenchloride; sulfuric acid; sodium nitrite; 1.1: Diazotization / 1.2: Substitution / 2.1: Oxidation;

DOI:10.1002/ps.2780410210

Reference yield:

→ 2.3.4-Trichlorbenzamid (24055-86-5)

Guidance literature:

2.3.4-Trichlorbenzoyl-chlorid, NH4OH, Ether;

upstream raw materials:

2,3,4-tri-chloro-benzonitrile

2,3,4-trichloroaniline

Downstream raw materials:

2,3,4-trichlorobenzoic acid

2,3,4-Trichlor-benzoylchlorid

Refernces