Multi-step reaction with 10 steps
1.1: copper(l) iodide / N,N-dimethyl-formamide / 5 h / 100 °C / Sealed vessel
2.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.03 h / 0 °C
2.2: 1 h / 20 °C
3.1: hydrazine hydrate / 1,4-dioxane; water / 0.5 h / 160 °C / Microwave irradiation
4.1: triethylamine / dichloromethane / 0.33 h / 0 °C
5.1: trichlorophosphate / acetonitrile / 0.17 h / 150 °C / Microwave irradiation
6.1: sodium hydrogencarbonate / tetrakis(triphenylphosphine) palladium(0) / 1,4-dioxane; water / 0.22 h / 150 °C / Microwave irradiation
7.1: osmium(VIII) oxide; sodium periodate / 1,4-dioxane; water; tert-butyl alcohol / 2 h / 20 °C
8.1: sodium tetrahydroborate / methanol / 1 h / 0 - 20 °C
9.1: triethylamine / dichloromethane / 2 h / 0 - 20 °C
10.1: N-ethyl-N,N-diisopropylamine; sodium iodide / acetonitrile / 3.5 h / 90 °C / Sealed vessel
With
sodium tetrahydroborate; sodium periodate; copper(l) iodide; osmium(VIII) oxide; sodium hydride; sodium hydrogencarbonate; hydrazine hydrate; triethylamine; N-ethyl-N,N-diisopropylamine; sodium iodide; trichlorophosphate;
tetrakis(triphenylphosphine) palladium(0);
In
1,4-dioxane; methanol; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile; mineral oil; tert-butyl alcohol;