(N,N-DiMethylaMinoMethyl)styrene

Base Information

• Chemical Name: (N,N-DiMethylaMinoMethyl)styrene
• CAS No.: 22826-55-7
• Molecular Formula: C11H15N
• Molecular Weight: 161.247
• Mol file: 22826-55-7.mol

Synonyms:(N,N-DiMethylaMinoMethyl)styrene

Chemical Property of (N,N-DiMethylaMinoMethyl)styrene

Chemical Property:

• Boiling Point: 212.9 °C at 760 mmHg
• PKA: 8.69±0.28(Predicted)
• Flash Point: 74.7 °C
• PSA: 3.24000
• Density: 0.937 g/cm³
• LogP: 2.39120
• Storage Temp.: 2-8°C

Purity/Quality:

95% ^*data from raw suppliers

N,N-Dimethyl-1-(2-vinylphenyl)methanamine 95+% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Uses: (N,N-DiMethylaMinoMethyl)styrene is an amine derivative and can be used as a pharmaceutical intermediate for pharmaceutical synthesis and pharmaceutical experimental research.

Technology Process of (N,N-DiMethylaMinoMethyl)styrene

There total 16 articles about (N,N-DiMethylaMinoMethyl)styrene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

[Ru(η6-C6H6)(2-N,N-dimethylbenzylamine(-1H))(MeCN)]PF6 → [(η6-benzene)Ru(CHMeC6H4CH2NMe2)(NCMe)]PF6 + N,N-dimethylaminomethylstyrene (22826-55-7)

Guidance literature:

With ethene; In methanol; stirred, room temp., under 1.5 bar of ethylene over 1.5 h;

DOI:10.1039/a908703f

Reference yield: 81.0%

ethene (74-85-1) → N,N-dimethylaminomethylstyrene (22826-55-7)

Guidance literature:

In methanol; at 20 ℃; for 1.5h; under 1125.09 Torr;

DOI:10.1039/a908703f

Reference yield: 52.0%

2,2-dimethyl-1,2,3,4-tetrahydroisoquinolinium iodide (1637-45-2) → N,N-dimethylaminomethylstyrene (22826-55-7)

Guidance literature:

With silver(l) oxide; In water; for 1h;

upstream raw materials:

2,2-dimethyl-1,2,3,4-tetrahydro-isoquinolinium; chloride

2,2-dimethyl-1,2,3,4-tetrahydroisoquinolinium iodide

2,2-dimethyl-4-(trimethylsilyl)-1,2,3,4-tetrahydroisoquinolinium iodide

2-methyl-2-<(trimethylsilyl)methyl>-1,2,3,4-tetrahydroisoquinolinium iodide

Downstream raw materials:

2--benzhydrol

1-(2-benzylphenyl)-N,N-dimethylmethanamine

2-chloromethylstyrene

NCNMe₂

Refernces

• 1、 -. "GROUP 8 TRANSITION METAL CATALYSTS AND METHOD FOR MAKING SAME AND PROCESS FOR USE OF SAME IN OLEFIN DISPROPORTIONATION REACTIONS". Page/Page column 34-35; 38. . Retrieved 2017/12/09.
• 2、 Ritleng, Vincent,Sutter, Jean Pascal,Pfeffer, Michel,Sirlin, Claude. "Cycloruthenated tertiary amines and ethylene: Further insight to the Ru- mediated olefin-aryl coupling reaction". . p. 129 - 130. Retrieved 2007/10/03.