ethyl 4-nitro-2-hydroxybenzimidate

Base Information

• Chemical Name: ethyl 4-nitro-2-hydroxybenzimidate
• CAS No.: 747369-57-9
• Molecular Formula: C₉H₁₀N₂O₄
• Molecular Weight: 210.189
• Mol file: 747369-57-9.mol

Synonyms:

Chemical Property of ethyl 4-nitro-2-hydroxybenzimidate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of ethyl 4-nitro-2-hydroxybenzimidate

There total 1 articles about ethyl 4-nitro-2-hydroxybenzimidate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

ethanol (64-17-5) + 2-hydroxy-4-nitro-benzonitrile (39835-14-8) → ethyl 4-nitro-2-hydroxybenzimidate (747369-57-9)

Guidance literature:

With hydrogenchloride; diethyl ether;

DOI:10.1021/ja01147a006

Reference yield:

ethyl 4-nitro-2-hydroxybenzimidate (747369-57-9) → aminoparabactin (105430-56-6)

Guidance literature:

Multi-step reaction with 2 steps

1: 85 percent / methanol / 20 h / Heating

2: 89 percent / H₂ / 10percent Pd/C / ethanol / 6 h

With hydrogen; palladium on activated charcoal; In methanol; ethanol;

DOI:10.1021/jo00377a026

upstream raw materials:

ethanol

2-hydroxy-4-nitro-benzonitrile

Downstream raw materials:

aminoparabactin