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3β-tiboloyl (R)-2-methoxy-2-phenylpent-3-ynoate

Base Information Edit
  • Chemical Name:3β-tiboloyl (R)-2-methoxy-2-phenylpent-3-ynoate
  • CAS No.:1357075-91-2
  • Molecular Formula:C33H40O4
  • Molecular Weight:500.678
  • Hs Code.:
  • Mol file:1357075-91-2.mol
3β-tiboloyl (R)-2-methoxy-2-phenylpent-3-ynoate

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The product has achieved commercial mass production*data from LookChem market partment
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Chemical Property of 3β-tiboloyl (R)-2-methoxy-2-phenylpent-3-ynoate Edit
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Technology Process of 3β-tiboloyl (R)-2-methoxy-2-phenylpent-3-ynoate

There total 8 articles about 3β-tiboloyl (R)-2-methoxy-2-phenylpent-3-ynoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
With dmap; dicyclohexyl-carbodiimide; In dichloromethane; at 20 ℃; for 24h; diastereoselective reaction; Inert atmosphere;
DOI:10.1021/jo2016554
Guidance literature:
Multi-step reaction with 5 steps
1: tetrahydrofuran / 2 h / -78 °C / Inert atmosphere
2: sodium hydride / tetrahydrofuran; mineral oil / 2 h / 20 °C / Inert atmosphere
3: N-chloro-succinimide; silver nitrate / water; acetonitrile / 0.17 h / 0 °C / Inert atmosphere
4: Jones reagent / acetone / 1 h / 0 °C / Inert atmosphere
5: dmap; dicyclohexyl-carbodiimide / dichloromethane / 24 h / 20 °C / Inert atmosphere
With dmap; N-chloro-succinimide; Jones reagent; sodium hydride; silver nitrate; dicyclohexyl-carbodiimide; In tetrahydrofuran; dichloromethane; water; acetone; acetonitrile; mineral oil;
DOI:10.1021/jo2016554
Guidance literature:
Multi-step reaction with 4 steps
1: sodium hydride / tetrahydrofuran; mineral oil / 2 h / 20 °C / Inert atmosphere
2: N-chloro-succinimide; silver nitrate / water; acetonitrile / 0.17 h / 0 °C / Inert atmosphere
3: Jones reagent / acetone / 1 h / 0 °C / Inert atmosphere
4: dmap; dicyclohexyl-carbodiimide / dichloromethane / 24 h / 20 °C / Inert atmosphere
With dmap; N-chloro-succinimide; Jones reagent; sodium hydride; silver nitrate; dicyclohexyl-carbodiimide; In tetrahydrofuran; dichloromethane; water; acetone; acetonitrile; mineral oil;
DOI:10.1021/jo2016554
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