3,7-Dimethyl-6-octen-3-ol

Base Information

• Chemical Name: 3,7-Dimethyl-6-octen-3-ol
• CAS No.: 2270-57-7
• Molecular Formula: C10H20O
• Molecular Weight: 156.27
• Hs Code.: 2905290000
• Mol file: 2270-57-7.mol

Synonyms:3,7-Dimethyl-6-octen-3-ol;

Chemical Property of 3,7-Dimethyl-6-octen-3-ol

Chemical Property:

• Boiling Point: 223.7 °C at 760 mmHg
• Flash Point: 100.5 °C
• PSA: 20.23000
• Density: 0.846 g/cm³
• LogP: 2.89380

Purity/Quality:

99%, ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 3,7-Dimethyl-6-octen-3-ol

There total 32 articles about 3,7-Dimethyl-6-octen-3-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

3,7-dimethyloct-6-en-1-yn-3-ol (29171-20-8) → 3,7-dimethyloct-6-en-3-ol (57029-98-8,2270-57-7,94006-45-8) + (S)-(+)-linalool (126-90-9)

Guidance literature:

With hydrogen; In hexane; at 50 ℃; for 10h; under 760.051 Torr;

DOI:10.1002/anie.201207845

Reference yield: 99.0%

3,7-dimethylocta-1,6-dien-3-ol (78-70-6) → dihydrolinalool (18479-51-1,2270-57-7,94006-45-8)

Guidance literature:

With fac-[Mn(1,2-bis(di-isopropylphosphino)ethane)(CO)₃(CH₂CH₂CH₃)]; hydrogen; In diethyl ether; at 25 ℃; for 18h; under 37503.8 Torr;

DOI:10.1021/acscatal.9b03963

Reference yield: 94.0%

1-(1-Ethyl-1,5-dimethyl-hex-4-enyloxymethoxy)-4-methoxy-benzene (124068-47-9) → dihydrolinalool (18479-51-1,2270-57-7,94006-45-8)

Guidance literature:

With ammonium cerium(IV) nitrate; In water; acetonitrile; at 0 ℃; for 0.5h; Product distribution;

DOI:10.1246/cl.1999.659

upstream raw materials:

(2R,4R)-4-(1-Ethyl-1,5-dimethyl-hex-4-enyloxy)-pentan-2-ol

linalool

(S)-(+)-linalool

6-Methyl-hept-5-en-2-on

Downstream raw materials:

2,6-bis-benzylsulfanyl-2,6-dimethyl-octane

Refernces

• 1、 Naves. "". . . Retrieved 1948.
• 2、 Miyazaki, Masayoshi,Furukawa, Shinya,Komatsu, Takayuki. "Regio- and Chemoselective Hydrogenation of Dienes to Monoenes Governed by a Well-Structured Bimetallic Surface". . p. 18231 - 18239. Retrieved 2017/12/27.
• 3、 Gao, Shuiying,Cao, Minna,Li, Weijin,Cao, Rong. "Palladium nanoparticles in situ generated in metal-organic films for catalytic applications". . p. 12185 - 12193. Retrieved 2014/08/05.