1-(1-Naphthyliminomethyl)-2-naphthol

Base Information

• Chemical Name: 1-(1-Naphthyliminomethyl)-2-naphthol
• CAS No.: 29101-37-9
• Molecular Formula: C₂₁H₁₅NO
• Molecular Weight: 297.356
• European Community (EC) Number: 653-597-0
• Nikkaji Number: J2.264.825J,J716.146H
• Mol file: 29101-37-9.mol

Synonyms:1-(1-Naphthyliminomethyl)-2-naphthol;1-((Naphthalen-1-ylimino)methyl)naphthalen-2-ol;29101-37-9;1-[(E)-(naphthalen-1-ylimino)methyl]naphthalen-2-ol;134558-92-2;STK179843;AKOS001581388;EU-0099904;1-[(E)-[(naphthalen-1-yl)imino]methyl]naphthalen-2-ol;1-[[(1-Naphthyl)amino]methylene]naphthalene-2(1H)-one;N-(2-{[4-(2-methoxyphenyl)piperazin-1-yl]carbonyl}-1H-indol-3-yl)-3-methylbenzamide

Chemical Property of 1-(1-Naphthyliminomethyl)-2-naphthol

Chemical Property:

• Boiling Point: 526.8 °C at 760 mmHg
• Flash Point: 353.9 °C
• PSA: 32.59000
• Density: 1.15 g/cm³
• LogP: 5.44920
• XLogP3: 5.4
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 2
• Exact Mass: 297.115364102
• Heavy Atom Count: 23
• Complexity: 420

Purity/Quality:

98%,99%, ^*data from raw suppliers

1-(1-NAPHTHYLIMINOMETHYL)-2-NAPHTHOL AldrichCPR ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC=C2C(=C1)C=CC=C2N=CC3=C(C=CC4=CC=CC=C43)O

Technology Process of 1-(1-Naphthyliminomethyl)-2-naphthol

There total 4 articles about 1-(1-Naphthyliminomethyl)-2-naphthol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-amino-naphthalene (134-32-7) + 2-hydroxynaphthalene-1-carbaldehyde (708-06-5) → 2-hydroxynaphthalene-1-carbaldehydene-1-naphthylamine (29101-37-9)

Guidance literature:

durch Zusammenschmelzen;

Reference yield:

1-amino-naphthalene (134-32-7) → 2-hydroxynaphthalene-1-carbaldehydene-1-naphthylamine (29101-37-9)

Guidance literature:

With ethanol; durch Kochen;

Reference yield:

β-naphthol (135-19-3) → 2-hydroxynaphthalene-1-carbaldehydene-1-naphthylamine (29101-37-9)

Guidance literature:

Multi-step reaction with 2 steps

1: NaOH; water; alcohol / 65 - 70 °C / nach ca. 1 Stde_. destilliert man den Alkohol ab, saeuert stark mit Salzsaeure an und destilliert das Produkt im Vakuum

2: durch Zusammenschmelzen

With sodium hydroxide; ethanol; water;

upstream raw materials:

1-amino-naphthalene

2-hydroxynaphthalene-1-carbaldehyde

β-naphthol

Refernces

• 1、 Dutta, Jayita,Richmond, Michael G.,Bhattacharya, Samaresh. "Palladium(0)-mediated C-H bond activation of N-(naphthyl)salicylaldimine and related ligands: utilization of the resulting organopalladium complexes in catalytic C-C and C-N coupling reactions". . p. 13615 - 13632. Retrieved 2015/08/03.