1H,1H,2H,2H-Tridecafluorooctyl acetate

Base Information Edit

Chemical Name:1H,1H,2H,2H-Tridecafluorooctyl acetate
CAS No.:37858-03-0
Molecular Formula:C10H7F13O2
Molecular Weight:406.144
Hs Code.:2915390090
Mol file:37858-03-0.mol

Synonyms:1H,1H,2H,2H-Tridecafluorooctyl acetate;

Suppliers and Price of 1H,1H,2H,2H-Tridecafluorooctyl acetate

Supply Marketing:Edit

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 6 raw suppliers

Chemical Property of 1H,1H,2H,2H-Tridecafluorooctyl acetate Edit

Chemical Property:

Melting Point:-73 °C
Refractive Index:1.3215
Boiling Point:172 °C
Flash Point:66 °C
PSA：26.30000
Density:1.5515 g/cm³
LogP:4.67840

Purity/Quality:: 98%Min ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 1H,1H,2H,2H-Tridecafluorooctyl acetate

There total 3 articles about 1H,1H,2H,2H-Tridecafluorooctyl acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 647-42-7
1H,1H,2H,2H-tridecafluoro-n-octanol

: 75-36-5
acetyl chloride

: 37858-03-0
Acetic acid 3,3,4,4,5,5,6,6,7,7,8,8,8-tridecafluoro-octyl ester

Guidance literature:: With triethylamine; In dichloromethane; at 25 ℃; for 12h;
DOI:10.3390/90500266

Reference yield:

: 108-05-4,9003-20-7
vinyl acetate

: 355-43-1
n-perfluorohexyl iodide

: 56734-81-7
2H,2H-tridecafluoro-octanal

: 37858-03-0
Acetic acid 3,3,4,4,5,5,6,6,7,7,8,8,8-tridecafluoro-octyl ester

: 80705-17-5
1,4-bis(perfluorohexyl)butan-2,3-diol diacetate

: 142502-58-7
Acetic acid 3,3,4,4,5,5,6,6,7,7,8,8,8-tridecafluoro-1-iodo-octyl ester

Guidance literature:: With zinc; In neat (no solvent); at 25 ℃; for 5h;
DOI:10.1016/S0040-4039(00)92222-6

Reference yield:

: 830330-63-7
3-hydroxy-3-phenyl-propionic acid 3,3,4,4,5,5,6,6,7,7,8,8,8-tridecafluoro-octyl ester

: 37858-03-0
Acetic acid 3,3,4,4,5,5,6,6,7,7,8,8,8-tridecafluoro-octyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: LiHBEt₃ / tetrahydrofuran / 2 h / 20 °C

2: 78 percent / Et₃N / CH₂Cl₂ / 12 h / 25 °C

With lithium triethylborohydride; triethylamine; In tetrahydrofuran; dichloromethane;
DOI:10.3390/90500266