9-hydroxy-β-ionylideneacetaldehyde dimethyl acetal

Base Information

• Chemical Name: 9-hydroxy-β-ionylideneacetaldehyde dimethyl acetal
• CAS No.: 1224-76-6
• Molecular Formula: C₁₇H₃₀O₃
• Molecular Weight: 282.423
• Mol file: 1224-76-6.mol

Synonyms:

Chemical Property of 9-hydroxy-β-ionylideneacetaldehyde dimethyl acetal

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 9-hydroxy-β-ionylideneacetaldehyde dimethyl acetal

There total 1 articles about 9-hydroxy-β-ionylideneacetaldehyde dimethyl acetal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

→ 9-hydroxy-β-ionylideneacetaldehyde dimethyl acetal (1224-76-6)

Guidance literature:

Ethinylcarbinol III, LiAlH4;

Reference yield:

9-hydroxy-β-ionylideneacetaldehyde dimethyl acetal (1224-76-6) → 9Z,11E,13Z-12-carboxyretinoic acid (6703-19-1,81176-73-0,81176-74-1,99394-38-4)

Guidance literature:

Multi-step reaction with 2 steps

1: aq. HCl / acetone / 1.5 h / Heating

2: potassium hydroxide / methanol / 64 h / 20 °C

With hydrogenchloride; potassium hydroxide; In methanol; acetone;

Reference yield:

9-hydroxy-β-ionylideneacetaldehyde dimethyl acetal (1224-76-6) → 11-cis,13-cis-12-carboxyretinoic acid (81176-73-0)

Guidance literature:

Multi-step reaction with 2 steps

1: aq. HCl / acetone / 1.5 h / Heating

2: potassium hydroxide / methanol / 64 h / 20 °C

With hydrogenchloride; potassium hydroxide; In methanol; acetone;

Downstream raw materials:

(2E,4E)-3-methyl-5-(2,6,6-trimethyl-1-cyclohexen-1-yl)-2,4-pentadienal

(2Z,4E)-3-methyl-5-[2,6,6-trimethylcyclohex-1-enyl]penta-2,4-dienal

9Z,11E,13Z-12-carboxyretinoic acid

11-cis,13-cis-12-carboxyretinoic acid