Technology Process of 1-Chloro-3-(3,4-dichloro-phenyl)-indan
There total 7 articles about 1-Chloro-3-(3,4-dichloro-phenyl)-indan which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
thionyl chloride;
In
toluene;
1.) RT, 30 min, 2.) from 50 deg C to 55 deg C, 1 h;
DOI:10.1021/jm00361a002
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 1.) Mg / 1.) ether, 2.) ether, toluene, reflux, 30 min
2: aq. H2SO4, CH3COOH / 24 h / Heating
3: 91 percent / polyphosphoric acid (PPA) / 2 h / 100 °C
4: 76 percent / sodium borohydride / methanol / 1 h / Ambient temperature
5: SOCl2 / toluene / 1.) RT, 30 min, 2.) from 50 deg C to 55 deg C, 1 h
With
sodium tetrahydroborate; thionyl chloride; PPA; Polyphosphoric acid (PPA); sulfuric acid; magnesium; acetic acid;
In
methanol; toluene;
DOI:10.1021/jm00361a002
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 1.) Mg / 1.) ether, 2.) ether, toluene, reflux, 30 min
2: aq. H2SO4, CH3COOH / 24 h / Heating
3: 91 percent / polyphosphoric acid (PPA) / 2 h / 100 °C
4: 76 percent / sodium borohydride / methanol / 1 h / Ambient temperature
5: SOCl2 / toluene / 1.) RT, 30 min, 2.) from 50 deg C to 55 deg C, 1 h
With
sodium tetrahydroborate; thionyl chloride; PPA; Polyphosphoric acid (PPA); sulfuric acid; magnesium; acetic acid;
In
methanol; toluene;
DOI:10.1021/jm00361a002