racem.-4.4'.α.α'-tetrachloro-bibenzyl

Base Information

• Chemical Name: racem.-4.4'.α.α'-tetrachloro-bibenzyl
• CAS No.: 16740-47-9
• Molecular Formula: C₁₄H₁₀Cl₄
• Molecular Weight: 320.045
• Mol file: 16740-47-9.mol

Synonyms:

Chemical Property of racem.-4.4'.α.α'-tetrachloro-bibenzyl

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of racem.-4.4'.α.α'-tetrachloro-bibenzyl

There total 6 articles about racem.-4.4'.α.α'-tetrachloro-bibenzyl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(E)-1,2-di(4-chlorophenyl)ethene (2510-74-9,5121-74-4,1657-56-3,144606-14-4) → meso-4.4'.α.α'-tetrachloro-bibenzyl (16740-47-9) + racem.-4.4'.α.α'-tetrachloro-bibenzyl (16740-47-9,27872-13-5)

Guidance literature:

With tetrachloromethane; chlorine; at 20 ℃;

DOI:10.1021/jo01169a003

Reference yield:

(E)-1,2-di(4-chlorophenyl)ethene (2510-74-9,5121-74-4,1657-56-3,144606-14-4) → meso-4.4'.α.α'-tetrachloro-bibenzyl (16740-47-9) + racem.-4.4'.α.α'-tetrachloro-bibenzyl (16740-47-9,27872-13-5)

Guidance literature:

With tetrachloromethane; chlorine; at 20 ℃;

DOI:10.1021/jo01169a003

Reference yield:

1,1-Dichloro-2,2-bis(p-chlorophenyl)ethane (72-54-8) → meso-4.4'.α.α'-tetrachloro-bibenzyl (16740-47-9)

Guidance literature:

With iron(III) chloride; at 110 ℃;

DOI:10.1021/jo01169a003

upstream raw materials:

(E)-1,2-di(4-chlorophenyl)ethene

1,1-Dichloro-2,2-bis(p-chlorophenyl)ethane

racem.-4.4'.α.α'-tetrachloro-bibenzyl

iron(III) chloride