Technology Process of 1-Butanamine, 4-[(phenylmethyl)thio]-
There total 4 articles about 1-Butanamine, 4-[(phenylmethyl)thio]- which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1: potassium iodide; potassium carbonate / N,N-dimethyl-formamide / 10 h / 20 °C / Inert atmosphere
2: hydrazine hydrate / methanol / 4 h / 70 °C
With
potassium carbonate; hydrazine hydrate; potassium iodide;
In
methanol; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.5 h / 0 °C
1.2: 0 - 20 °C
2.1: hydrazine hydrate / methanol / 4 h / Inert atmosphere; Reflux
With
sodium hydride; hydrazine hydrate;
In
methanol; N,N-dimethyl-formamide; mineral oil;
- Guidance literature:
-
With
sodium hydroxide;
Erwaermen des Reaktionsprodukts mit wss. N2H4+H2O in Aethanol;