(Z)-5-decenyl triphenylphosphonium bromide

Base Information

• Chemical Name: (Z)-5-decenyl triphenylphosphonium bromide
• CAS No.: 64275-64-5
• Molecular Formula: Br*C₂₈H₃₄P
• Molecular Weight: 481.456
• Mol file: 64275-64-5.mol

Synonyms:

Chemical Property of (Z)-5-decenyl triphenylphosphonium bromide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (Z)-5-decenyl triphenylphosphonium bromide

There total 4 articles about (Z)-5-decenyl triphenylphosphonium bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

tetrahydro-2H-2-pyranol (694-54-2) → (Z)-5-decenyl triphenylphosphonium bromide (64275-64-5)

Guidance literature:

Multi-step reaction with 3 steps

1: NaH, DMSO

2: PBr₃, Py

3: xylene / Heating

With pyridine; phosphorus tribromide; sodium hydride; dimethyl sulfoxide; In xylene;

DOI:10.1002/hlca.19770600404

Reference yield:

(Z)-dec-5-en-1-ol (51652-47-2) → (Z)-5-decenyl triphenylphosphonium bromide (64275-64-5)

Guidance literature:

Multi-step reaction with 2 steps

1: PBr₃, Py

2: xylene / Heating

With pyridine; phosphorus tribromide; In xylene;

DOI:10.1002/hlca.19770600404

Reference yield:

pentyltriphenylphosphonium bromide (21406-61-1) → (Z)-5-decenyl triphenylphosphonium bromide (64275-64-5)

Guidance literature:

Multi-step reaction with 3 steps

1: NaH, DMSO

2: PBr₃, Py

3: xylene / Heating

With pyridine; phosphorus tribromide; sodium hydride; dimethyl sulfoxide; In xylene;

DOI:10.1002/hlca.19770600404

upstream raw materials:

1-bromo-dec-5c-ene

triphenylphosphine

tetrahydro-2H-2-pyranol

(Z)-dec-5-en-1-ol