N,N'-(Iminobisethylene)bismethanamine

Base Information

• Chemical Name: N,N'-(Iminobisethylene)bismethanamine
• CAS No.: 4432-89-7
• Molecular Formula: C6H17 N3
• Molecular Weight: 131.221
• Mol file: 4432-89-7.mol

Synonyms:1,2-Ethanediamine,N-methyl-N'-[2-(methylamino)ethyl]- (9CI); Diethylenetriamine, 1,7-dimethyl-(7CI,8CI); 1,7-Dimethyldiethylenetriamine; 2,5,8-Triazanonane;N,N''-Dimethyldiethylenetriamine

Chemical Property of N,N'-(Iminobisethylene)bismethanamine

Chemical Property:

• PSA: 112.20000
• LogP: -0.22470

Purity/Quality:

99%, ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of N,N'-(Iminobisethylene)bismethanamine

There total 1 articles about N,N'-(Iminobisethylene)bismethanamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

→ 1,7-dimethyldiethylenetriamine (4432-89-7) + N-methyl-ethane-1,2-diamine (109-81-9)

Guidance literature:

With ethanol; nickel; at 80 - 100 ℃; Hydrogenation;

DOI:10.1021/ja01337a046

Reference yield:

1,7-dimethyldiethylenetriamine (4432-89-7) → C20H24N3O2P (75403-50-8)

Guidance literature:

Multi-step reaction with 2 steps

1: 91 percent / toluene / 26 h / Heating

2: 24.3 percent / -78 °C

In toluene;

DOI:10.1021/ja00543a031

Reference yield:

1,7-dimethyldiethylenetriamine (4432-89-7) + C21H29ClO8 (1326318-76-6) → C69H101N3O24

Guidance literature:

With triethylamine; In chloroform; at 20 ℃; for 14h;

DOI:10.1021/acs.langmuir.8b01944

Downstream raw materials:

C₂₀H₂₄N₃O₂P