C₉H₉ClN₂S

Base Information

• Chemical Name: C₉H₉ClN₂S
• CAS No.: 1263798-26-0
• Molecular Formula: C₉H₉ClN₂S
• Molecular Weight: 212.703
• Mol file: 1263798-26-0.mol

Synonyms:

Chemical Property of C₉H₉ClN₂S

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₉H₉ClN₂S

There total 2 articles about C₉H₉ClN₂S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-[(2-amino-3-chlorophenyl)dithio]-6-chlorophenylamine (63755-08-8) + acrylonitrile (107-13-1,25014-41-9) → C9H9ClN2S (1263798-26-0)

Guidance literature:

With ammonium thioglycolate; In N,N-dimethyl-formamide; at 50 ℃; Inert atmosphere;

DOI:10.3987/COM-10-12100

Reference yield:

4-chlorobenzo[d]thiazol-2-amine (19952-47-7) → C9H9ClN2S (1263798-26-0)

Guidance literature:

Multi-step reaction with 2 steps

1: potassium hydroxide / water; ethylene glycol / 140 °C / Reflux

2: ammonium thioglycolate / N,N-dimethyl-formamide / 50 °C / Inert atmosphere

With ammonium thioglycolate; potassium hydroxide; In water; ethylene glycol; N,N-dimethyl-formamide; 2: Michael condensation;

DOI:10.3987/COM-10-12100

upstream raw materials:

4-chlorobenzo[d]thiazol-2-amine

2-[(2-amino-3-chlorophenyl)dithio]-6-chlorophenylamine

acrylonitrile

Refernces