N-Pentafluorosulfanyl-N-nitro-2,4,6-trinitrobenzyl carbamate

Base Information

• Chemical Name: N-Pentafluorosulfanyl-N-nitro-2,4,6-trinitrobenzyl carbamate
• CAS No.: 136397-71-2
• Molecular Formula: C₈H₄F₅N₅O₁₀S
• Molecular Weight: 457.205
• Mol file: 136397-71-2.mol

Synonyms:

Chemical Property of N-Pentafluorosulfanyl-N-nitro-2,4,6-trinitrobenzyl carbamate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N-Pentafluorosulfanyl-N-nitro-2,4,6-trinitrobenzyl carbamate

There total 2 articles about N-Pentafluorosulfanyl-N-nitro-2,4,6-trinitrobenzyl carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N-Pentafluorosulfanyl-2,4,6-trinitrobenzyl carbamate (136397-67-6) → N-Pentafluorosulfanyl-N-nitro-2,4,6-trinitrobenzyl carbamate (136397-71-2)

Guidance literature:

With nitric acid; trifluoroacetic anhydride; at 0 ℃; for 2h;

DOI:10.1016/S0022-1139(00)80135-9

Reference yield:

2,4,6-trinitrobenzyl alcohol (24577-68-2) → N-Pentafluorosulfanyl-N-nitro-2,4,6-trinitrobenzyl carbamate (136397-71-2)

Guidance literature:

Multi-step reaction with 2 steps

1: 100 percent / acetonitrile / a.) -78 deg C to r.t., b.) r.t., 4h

2: 41 percent Spectr_. / 100percent nitric acid, trifluoroacetic anhydride / 2 h / 0 °C

With nitric acid; trifluoroacetic anhydride; In acetonitrile;

DOI:10.1016/S0022-1139(00)80135-9

upstream raw materials:

N-Pentafluorosulfanyl-2,4,6-trinitrobenzyl carbamate

2,4,6-trinitrobenzyl alcohol

Refernces