C₂₂H₂₄O₇

Base Information

• Chemical Name: C₂₂H₂₄O₇
• CAS No.: 1381843-18-0
• Molecular Formula: C₂₂H₂₄O₇
• Molecular Weight: 400.428
• Mol file: 1381843-18-0.mol

Synonyms:

Chemical Property of C₂₂H₂₄O₇

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₂H₂₄O₇

There total 6 articles about C₂₂H₂₄O₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

C15H16O5 + (1R,4R,5S)-(+)-4-hydroxy-6,6-dimethyl-3-oxabicyclo<3.1.0>hexan-2-one (2102-46-7,26771-21-1,67528-54-5,72937-63-4,79026-47-4,79082-71-6,99297-25-3,73611-02-6) → C22H24O7 (1381843-18-0) + C22H24O7 (1381843-39-5) + C22H24O7 (1381843-47-5)

Guidance literature:

With toluene-4-sulfonic acid; In benzene; for 1h; Reflux;

DOI:10.1016/j.mencom.2012.05.002

Reference yield:

C21H34O6Si (1381843-06-6) → C22H24O7 (1381843-18-0) + C22H24O7 (1381843-47-5)

Guidance literature:

Multi-step reaction with 2 steps

1: pyridinium p-toluenesulfonate / 1 h / 60 °C

2: toluene-4-sulfonic acid / benzene / 1 h / Reflux

With pyridinium p-toluenesulfonate; toluene-4-sulfonic acid; In benzene;

DOI:10.1016/j.mencom.2012.05.002

Reference yield:

C21H34O6Si (1381843-12-4) → C22H24O7 (1381843-18-0) + C22H24O7 (1381843-47-5)

Guidance literature:

Multi-step reaction with 2 steps

1: pyridinium p-toluenesulfonate / 1 h / 60 °C

2: toluene-4-sulfonic acid / benzene / 1 h / Reflux

With pyridinium p-toluenesulfonate; toluene-4-sulfonic acid; In benzene;

DOI:10.1016/j.mencom.2012.05.002

upstream raw materials:

C₂₁H₃₄O₆Si

C₂₁H₃₄O₆Si

C₂₄H₄₀O₆Si

C₂₄H₄₀O₆Si

Refernces