Technology Process of 7,10-dichloro-4-phenyl-2-t-butyl-5H-6-oxa-1-azaphenanthrene
There total 4 articles about 7,10-dichloro-4-phenyl-2-t-butyl-5H-6-oxa-1-azaphenanthrene which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 35 percent / NaH / dimethylformamide / 2 h / 100 °C
2: 1.) SOCl2, 2.) AlCl3 / 1.) 100 degC, 10 min, 2.)nitrobenzene, 20 degC, 48 h
3: 70 percent / 5 h / 100 °C
4: 1.) aqueous NH3, 2.) AcOH / 1.) Et2O, 20 degC, 1h, 2.) 16h
With
ammonium hydroxide; aluminium trichloride; thionyl chloride; sodium hydride; acetic acid;
In
N,N-dimethyl-formamide;
- Guidance literature:
-
With
ammonium hydroxide; acetic acid;
Yield given. Multistep reaction;
1.) Et2O, 20 degC, 1h, 2.) 16h;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 1.) SOCl2, 2.) AlCl3 / 1.) 100 degC, 10 min, 2.)nitrobenzene, 20 degC, 48 h
2: 70 percent / 5 h / 100 °C
3: 1.) aqueous NH3, 2.) AcOH / 1.) Et2O, 20 degC, 1h, 2.) 16h
With
ammonium hydroxide; aluminium trichloride; thionyl chloride; acetic acid;
