4,4,6-trimethyl-2,2-bis(4-methoxyphenyl)-1,3-dioxa-4-azonia-2-boratacyclohexane

Base Information

• Chemical Name: 4,4,6-trimethyl-2,2-bis(4-methoxyphenyl)-1,3-dioxa-4-azonia-2-boratacyclohexane
• CAS No.: 95890-43-0
• Molecular Formula: C₁₉H₂₆BNO₄
• Molecular Weight: 343.231
• Mol file: 95890-43-0.mol

Synonyms:

Chemical Property of 4,4,6-trimethyl-2,2-bis(4-methoxyphenyl)-1,3-dioxa-4-azonia-2-boratacyclohexane

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 4,4,6-trimethyl-2,2-bis(4-methoxyphenyl)-1,3-dioxa-4-azonia-2-boratacyclohexane

There total 1 articles about 4,4,6-trimethyl-2,2-bis(4-methoxyphenyl)-1,3-dioxa-4-azonia-2-boratacyclohexane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

DPB025 (37763-62-5) + N-(2-hydroxypropyl)-N,N-dimethylamine N-oxide (27607-29-0) → 4,4,6-trimethyl-2,2-bis(4-methoxyphenyl)-1,3-dioxa-4-azonia-2-boratacyclohexane (95890-43-0)

Guidance literature:

In ethanol; a mixt. of EtOH soln. of amine oxide and 1 equiv of borane in EtOH was refluxed for 15 min; cooled, resulting crystals (soln. was concd. if necessary) were sepd., recrystd. from EtOH-petroleum ether; elem. anal.;

DOI:10.1016/0022-328X(84)80698-1

upstream raw materials:

DPB₀₂₅

N-(2-hydroxypropyl)-N,N-dimethylamine N-oxide

Refernces