Technology Process of C43H39NOS4
There total 3 articles about C43H39NOS4 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
bis-triphenylphosphine-palladium(II) chloride;
In
N,N-dimethyl-formamide;
for 4h;
Inert atmosphere;
Reflux;
DOI:10.1039/c1jm12181b
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: n-butyllithium / tetrahydrofuran / Inert atmosphere
1.2: 0 - 20 °C / Inert atmosphere
1.3: 6 h / Inert atmosphere; Reflux
2.1: N-Bromosuccinimide; acetic acid / chloroform / 1 h / Inert atmosphere; Reflux
3.1: bis-triphenylphosphine-palladium(II) chloride / N,N-dimethyl-formamide / 4 h / Inert atmosphere; Reflux
With
bis-triphenylphosphine-palladium(II) chloride; N-Bromosuccinimide; n-butyllithium; acetic acid;
In
tetrahydrofuran; chloroform; N,N-dimethyl-formamide;
DOI:10.1039/c1jm12181b
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: n-butyllithium / tetrahydrofuran / Inert atmosphere
1.2: 0 - 20 °C / Inert atmosphere
1.3: 6 h / Inert atmosphere; Reflux
2.1: N-Bromosuccinimide; acetic acid / chloroform / 1 h / Inert atmosphere; Reflux
3.1: bis-triphenylphosphine-palladium(II) chloride / N,N-dimethyl-formamide / 4 h / Inert atmosphere; Reflux
With
bis-triphenylphosphine-palladium(II) chloride; N-Bromosuccinimide; n-butyllithium; acetic acid;
In
tetrahydrofuran; chloroform; N,N-dimethyl-formamide;
DOI:10.1039/c1jm12181b