11-cis-Vitamin-A⁽²⁾-p-phenylazobenzoat

Base Information

• Chemical Name: 11-cis-Vitamin-A⁽²⁾-p-phenylazobenzoat
• CAS No.: 124130-50-3
• Molecular Formula: C₃₃H₃₆N₂O₂
• Molecular Weight: 492.661
• Mol file: 124130-50-3.mol

Synonyms:

Chemical Property of 11-cis-Vitamin-A⁽²⁾-p-phenylazobenzoat

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 11-cis-Vitamin-A⁽²⁾-p-phenylazobenzoat

There total 41 articles about 11-cis-Vitamin-A⁽²⁾-p-phenylazobenzoat which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(Z)-3-methylpent-2-en-4-ynol (6153-05-5,105-29-3) → 11,13-Di-cis-vitamin-A(2)-p-phenylazobenzoat (124130-50-3)

Guidance literature:

Multi-step reaction with 3 steps

2: H₂, quinoline / Lindlar catalyst / petroleum ether

3: Py / benzene

With pyridine; quinoline; hydrogen; Lindlar's catalyst; In Petroleum ether; benzene;

DOI:10.1002/hlca.19620450215

Reference yield:

(E)-3-methylpent-2-en-4-yn-1-ol (6153-06-6,105-29-3) → 11-cis-Vitamin-A(2)-p-phenylazobenzoat (124130-50-3)

Guidance literature:

Multi-step reaction with 3 steps

2: H₂, quinoline / Lindlar catalyst / petroleum ether; ethyl acetate

3: Py / benzene

With pyridine; quinoline; hydrogen; Lindlar's catalyst; In ethyl acetate; Petroleum ether; benzene;

DOI:10.1002/hlca.19620450215

Reference yield:

(E)-2-Methyl-4-(2,6,6-trimethyl-cyclohexa-1,3-dienyl)-but-2-enal (100862-93-9) → 11,13-Di-cis-vitamin-A(2)-p-phenylazobenzoat (124130-50-3)

Guidance literature:

Multi-step reaction with 3 steps

2: H₂, quinoline / Lindlar catalyst / petroleum ether

3: Py / benzene

With pyridine; quinoline; hydrogen; Lindlar's catalyst; In Petroleum ether; benzene;

DOI:10.1002/hlca.19620450215

upstream raw materials:

4-phenylazobenzoyl chloride

vitamin A₂

(Z)-3-methylpent-2-en-4-ynol

(2E,4E)-3-methyl-5-(2,6,6-trimethylcyclohex-1-enyl)penta-2,4-dienoic acid