(+/-)-4-isopropyl-cyclohex-2-enone semicarbazone

Base Information

• Chemical Name: (+/-)-4-isopropyl-cyclohex-2-enone semicarbazone
• CAS No.: 4581-63-9
• Molecular Formula: C₁₀H₁₇N₃O
• Molecular Weight: 195.264
• Mol file: 4581-63-9.mol

Synonyms:

Chemical Property of (+/-)-4-isopropyl-cyclohex-2-enone semicarbazone

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (+/-)-4-isopropyl-cyclohex-2-enone semicarbazone

There total 3 articles about (+/-)-4-isopropyl-cyclohex-2-enone semicarbazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-methoxy-4-(1'-methylethyl)cyclohexa-1,4-diene (99180-72-0) + semicarbazide hydrochloride (563-41-7) → (+/-)-4-isopropyl-cyclohex-2-enone semicarbazone (4581-63-9)

Guidance literature:

With methanol;

DOI:10.1021/ja01609a060

Reference yield:

(R)-(-)-cryptone (2158-59-0) → (+/-)-4-isopropyl-cyclohex-2-enone semicarbazone (4581-63-9)

Guidance literature:

Multi-step reaction with 2 steps

1: diethyl ether; concentrated aqueous hydrochloric acid

With hydrogenchloride; diethyl ether;

DOI:10.1039/jr9390001531

Reference yield:

cryptone (2158-59-0,2158-61-4,100295-52-1,500-02-7) → (+/-)-4-isopropyl-cyclohex-2-enone semicarbazone (4581-63-9)

Guidance literature:

DOI:10.1039/jr9390001415 DOI:10.1039/jr9390001531

upstream raw materials:

1-methoxy-4-(1'-methylethyl)cyclohexa-1,4-diene

semicarbazide hydrochloride

cryptone

(R)-(-)-cryptone