Technology Process of 2-phenyl-4-formyl-5-methylmercaptothiazole
There total 5 articles about 2-phenyl-4-formyl-5-methylmercaptothiazole which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
sodium methylate;
In
methanol;
for 2h;
Heating;
DOI:10.1007/BF00475385
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 1.) phosphorus trichloride, 2.) phosphorus oxychloride / 1.) diethyl ether, 20 deg C, 30 min, 2.) 100 deg C, 7 h.
2: 90 percent / potassium hydrosulfide / H2O; methanol / 2 h / Heating
3: 64 percent / sodium methoxide / methanol / 2 h / Heating
With
sodium methylate; potassium hydrosulfide; trichlorophosphate; phosphorus trichloride;
In
methanol; water;
DOI:10.1007/BF00475385
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 90 percent / potassium hydrosulfide / H2O; methanol / 2 h / Heating
2: 64 percent / sodium methoxide / methanol / 2 h / Heating
With
sodium methylate; potassium hydrosulfide;
In
methanol; water;
DOI:10.1007/BF00475385
