1,2,3,3-tetrachloro-1,1,2-trifluoropropane

Base Information

• Chemical Name: 1,2,3,3-tetrachloro-1,1,2-trifluoropropane
• CAS No.: 422-41-3
• Molecular Formula: C₃HCl₄F₃
• Molecular Weight: 235.848
• Mol file: 422-41-3.mol

Synonyms:1,2,3,3-Tetrachloro-1,1,2-trifluoropropane;2,3,3-Trifluoro-1,1,2,3-tetrachloropropane; NSC 68378

Chemical Property of 1,2,3,3-tetrachloro-1,1,2-trifluoropropane

Chemical Property:

• Vapor Pressure: 11.8mmHg at 25°C
• Boiling Point: 130.6°C at 760 mmHg
• Flash Point: 39.7°C
• Density: 1.679g/cm³

Purity/Quality:

99%min ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1,2,3,3-tetrachloro-1,1,2-trifluoropropane

There total 7 articles about 1,2,3,3-tetrachloro-1,1,2-trifluoropropane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

1,1,1,2,3-pentachloro-2,3,3-trifluoro-propane (2354-05-4) → 1,2,3,3-tetrachloro-1,1,2-trifluoro-propane (422-41-3)

Guidance literature:

With isopropyl alcohol; for 6h; Ambient temperature; Irradiation;

DOI:10.1016/S0022-1139(97)00083-3

Reference yield:

1,1,1,2,2,3,3-heptachloropropane (594-89-8) + antimony(III) fluoride (7783-56-4) + chlorine (7782-50-5) → 1,2,3,3-tetrachloro-1,1,2-trifluoro-propane (422-41-3) + 1,1,2,2,3-pentachloro-3,3-difluoropropane (422-30-0) + 1,1,2,2,3,3-hexachloro-1-fluoro-propane (422-28-6)

Guidance literature:

at 130 - 150 ℃; je nach der Menge des Fluorierungsmittels Produkt₁ oder Produkt₂;

Reference yield:

1,1,1,2,2,3,3-heptachloropropane (594-89-8) → 1,2,3,3-tetrachloro-1,1,2-trifluoro-propane (422-41-3)

Guidance literature:

With antimony(III) fluoride; chlorine; at 140 - 150 ℃;

upstream raw materials:

1,1,2,2,3-pentachloro-3,3-difluoropropane

chloroform

Chlorotrifluoroethylene

1,1,1,2,2,3,3-heptachloropropane

Downstream raw materials:

1,1,1,2,3-pentachloro-2,3,3-trifluoro-propane

Refernces

• 1、 Paleta, Oldrich,Kvicala, Jaroslav,Guenter, Jaroslav,Dedek, Vaclav. "Synthesis of > and Some Chlorofluoropropenes". . p. 920 - 924. Retrieved 2007/10/02.