Cr(C₂₃H₃₂NO)2

Base Information

• Chemical Name: Cr(C₂₃H₃₂NO)2
• CAS No.: 223414-18-4
• Molecular Formula: C₄₆H₆₄CrN₂O₂
• Molecular Weight: 729.022
• Mol file: 223414-18-4.mol

Synonyms:

Chemical Property of Cr(C₂₃H₃₂NO)2

Chemical Property:

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Technology Process of Cr(C₂₃H₃₂NO)2

There total 1 articles about Cr(C₂₃H₃₂NO)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

2,6-Me2-C6H4NHCH2(3,5-(t)Bu2-C6H2-2-OH) (223414-21-9) + trichlorotris(tetrahydrofuran)chromium(III) (10170-68-0,16997-54-9) → Cr(C23H32NO)2 (223414-18-4)

Guidance literature:

With n-BuLi; In tetrahydrofuran; addn. of n-BuLi to org. ligand in THF at -78°C, warming to room temp., stirring (1 h), cooling to -78°C, addn. of CrCl3(THF)3, warming to room temp., stirring (12 h); removal of volatiles, extn. (pentane), evapn., recrystn. (heptane, standing at ambient temp., 1-2 d); elem. anal.;

upstream raw materials:

2,6-Me₂-C₆H₄NHCH₂(3,5-(t)Bu₂-C₆H₂-2-OH)

trichlorotris(tetrahydrofuran)chromium(III)

Refernces