1-(4-hydroxymethyl-benzyl)-8,15,22-trimethyl-1,8,15,22-triazonia-tricyclo(13.13.6.6^8,22)tetracontane tetracation

Base Information

• Chemical Name: 1-(4-hydroxymethyl-benzyl)-8,15,22-trimethyl-1,8,15,22-triazonia-tricyclo(13.13.6.6^8,22)tetracontane tetracation
• CAS No.: 105183-16-2
• Molecular Formula: C₄₇H₉₀N₄O
• Molecular Weight: 727.258
• Mol file: 105183-16-2.mol

Synonyms:

Chemical Property of 1-(4-hydroxymethyl-benzyl)-8,15,22-trimethyl-1,8,15,22-triazonia-tricyclo(13.13.6.6^8,22)tetracontane tetracation

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1-(4-hydroxymethyl-benzyl)-8,15,22-trimethyl-1,8,15,22-triazonia-tricyclo(13.13.6.6^8,22)tetracontane tetracation

There total 2 articles about 1-(4-hydroxymethyl-benzyl)-8,15,22-trimethyl-1,8,15,22-triazonia-tricyclo(13.13.6.6^8,22)tetracontane tetracation which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-(4-carboxybenzyl)-8,15,22-trimethyl-1,8,15,22-tetrazoniatricyclo<13.13.6.68,22>tetracontane tetrakis(tetrafluoroborate) (105206-52-8) → 1-(4-hydroxymethyl-benzyl)-8,15,22-trimethyl-1,8,15,22-triazonia-tricyclo(13.13.6.68,22)tetracontane tetracation (105183-16-2)

Guidance literature:

With dimethylsulfide borane complex; In nitromethane;

DOI:10.1016/S0040-4039(00)84428-7

Reference yield:

4-(bromomethyl)benzyl alcohol (71831-21-5) + C39H81N4(3+) (127056-24-0) → 1-(4-hydroxymethyl-benzyl)-8,15,22-trimethyl-1,8,15,22-triazonia-tricyclo(13.13.6.68,22)tetracontane tetracation (105183-16-2)

Guidance literature:

Yield given;

DOI:10.1016/S0040-4039(00)82313-8

Reference yield:

1-(4-hydroxymethyl-benzyl)-8,15,22-trimethyl-1,8,15,22-triazonia-tricyclo(13.13.6.68,22)tetracontane tetracation (105183-16-2) → 1-(4-(bromomethyl)benzyl)-8,15,22-trimethyl-1,8,15,22-tetrazoniatricyclo<13.13.6.6.8,22>tetracontane tetrakis(tetrafluoroborate)

Guidance literature:

With hydrogen bromide; In water; Yield given;

DOI:10.1016/S0040-4039(00)84428-7

upstream raw materials:

4-(bromomethyl)benzyl alcohol

C₃₉H₈₁N₄⁽³⁺⁾

1-(4-carboxybenzyl)-8,15,22-trimethyl-1,8,15,22-tetrazoniatricyclo<13.13.6.6^8,22>tetracontane tetrakis(tetrafluoroborate)

Refernces

• 1、 Bergmann, N.,Schmidtchen, F. P.. "A NOVEL ENZYME MIMIC FOR THIAZOLIUM-CATALYZED α-KETOACID DECARBOXYLATION". . p. 6235 - 6238. Retrieved 2007/10/02.