(1S,2R)-2-methylcyclohexanethiol

Base Information

• Chemical Name: (1S,2R)-2-methylcyclohexanethiol
• CAS No.: 22425-07-6
• Molecular Formula: C₇H₁₄S
• Molecular Weight: 130.254
• Mol file: 22425-07-6.mol

Synonyms:

Chemical Property of (1S,2R)-2-methylcyclohexanethiol

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (1S,2R)-2-methylcyclohexanethiol

There total 4 articles about (1S,2R)-2-methylcyclohexanethiol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-methylcyclohex-1-ene (591-49-1) → (+/-)-trans-1-methyl-cyclohexanethiol-(2) (22425-07-6,99419-74-6)

Guidance literature:

With acetone; at 0 ℃; Einwirkung von UV-Licht;

DOI:10.1039/jr9470001532

Reference yield:

1-methylcyclohex-1-ene (591-49-1) + thioacetic acid (507-09-5) → (+/-)-cis-1-methyl-cyclohexanethiol-(2) (22425-07-6)

Guidance literature:

Einwirkung von Licht, Aufteilung des erhaltenen Gemisches der stereoisomeren Thioessigsaeure-S-<2-methyl-cyclohexylester> durch fraktionierte Destillation und anschliessendes Kochen mit wss.-aethanol. KOH;

DOI:10.1039/jr9470000134 DOI:10.1021/ja01570a051

Reference yield:

1-methylcyclohex-1-ene (591-49-1) + thioacetic acid (507-09-5) → (+/-)-trans-1-methyl-cyclohexanethiol-(2) (22425-07-6,99419-74-6) + (+/-)-cis-1-methyl-cyclohexanethiol-(2) (22425-07-6)

Guidance literature:

Einwirkung von Licht, Aufteilung des erhaltenen Gemisches der stereoisomeren Thioessigsaeure-S-<2-methyl-cyclohexylester> durch fraktionierte Destillation und anschliessendes Kochen mit wss.-aethanol. KOH;

DOI:10.1021/ja01570a051

upstream raw materials:

1-methylcyclohex-1-ene

thioacetic acid