Technology Process of 2-(4-methoxyphenyl)-3-phenylquinolin-4(1H)-one
There total 4 articles about 2-(4-methoxyphenyl)-3-phenylquinolin-4(1H)-one which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
di-tert-butyl peroxide; iron(III) p-toluenesulfonate hexahydrate;
In
dimethyl sulfoxide;
at 110 ℃;
for 20h;
Sealed tube;
Inert atmosphere;
DOI:10.1021/acs.orglett.0c03011
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: magnesium; iodine / tetrahydrofuran / 1.5 h / 60 °C / Sealed tube
1.2: 20 °C / Sealed tube
1.3: pH 1
2.1: iron(III) p-toluenesulfonate hexahydrate; di-tert-butyl peroxide / dimethyl sulfoxide / 20 h / 110 °C / Sealed tube; Inert atmosphere
With
di-tert-butyl peroxide; iron(III) p-toluenesulfonate hexahydrate; iodine; magnesium;
In
tetrahydrofuran; dimethyl sulfoxide;
DOI:10.1021/acs.orglett.0c03011
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: magnesium; iodine / tetrahydrofuran / 1.5 h / 60 °C / Sealed tube
1.2: 20 °C / Sealed tube
1.3: pH 1
2.1: iron(III) p-toluenesulfonate hexahydrate; di-tert-butyl peroxide / dimethyl sulfoxide / 20 h / 110 °C / Sealed tube; Inert atmosphere
With
di-tert-butyl peroxide; iron(III) p-toluenesulfonate hexahydrate; iodine; magnesium;
In
tetrahydrofuran; dimethyl sulfoxide;
DOI:10.1021/acs.orglett.0c03011