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(+/-)-2-[2-(diphenylphosphino)phenyl]-5,6-dihydro-4-phenyl-4H-1,3-oxazine

Base Information Edit
  • Chemical Name:(+/-)-2-[2-(diphenylphosphino)phenyl]-5,6-dihydro-4-phenyl-4H-1,3-oxazine
  • CAS No.:292140-03-5
  • Molecular Formula:C28H24NOP
  • Molecular Weight:421.478
  • Hs Code.:
  • Mol file:292140-03-5.mol
(+/-)-2-[2-(diphenylphosphino)phenyl]-5,6-dihydro-4-phenyl-4H-1,3-oxazine

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Suppliers and Price of (+/-)-2-[2-(diphenylphosphino)phenyl]-5,6-dihydro-4-phenyl-4H-1,3-oxazine
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The product has achieved commercial mass production*data from LookChem market partment
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Chemical Property of (+/-)-2-[2-(diphenylphosphino)phenyl]-5,6-dihydro-4-phenyl-4H-1,3-oxazine Edit
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Technology Process of (+/-)-2-[2-(diphenylphosphino)phenyl]-5,6-dihydro-4-phenyl-4H-1,3-oxazine

There total 3 articles about (+/-)-2-[2-(diphenylphosphino)phenyl]-5,6-dihydro-4-phenyl-4H-1,3-oxazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
Multi-step reaction with 2 steps
1: 89 percent / NaBH4; cc. H2SO4 / tetrahydrofuran; diethyl ether / 0 - 20 °C
2: 28 percent / ZnCl2 / chlorobenzene / 94 h / Heating
With sodium tetrahydroborate; sulfuric acid; zinc(II) chloride; In tetrahydrofuran; diethyl ether; chlorobenzene; 1: Reduction / 2: alcoholysis;
DOI:10.1002/1522-2675(20000607)83:6<1256::AID-HLCA1256>3.0.CO;2-5
Guidance literature:
Multi-step reaction with 3 steps
1: 34 percent / AcONH4 / ethanol / 6 h / Heating
2: 89 percent / NaBH4; cc. H2SO4 / tetrahydrofuran; diethyl ether / 0 - 20 °C
3: 28 percent / ZnCl2 / chlorobenzene / 94 h / Heating
With sodium tetrahydroborate; sulfuric acid; ammonium acetate; zinc(II) chloride; In tetrahydrofuran; diethyl ether; ethanol; chlorobenzene; 1: Condensation / 2: Reduction / 3: alcoholysis;
DOI:10.1002/1522-2675(20000607)83:6<1256::AID-HLCA1256>3.0.CO;2-5
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