anhydromesaconitine trifluoromethanesulfonate

Base Information

• Chemical Name: anhydromesaconitine trifluoromethanesulfonate
• CAS No.: 86817-64-3
• Molecular Formula: C₃₄H₄₂F₃NO₁₂S
• Molecular Weight: 745.768
• Mol file: 86817-64-3.mol

Synonyms:

Chemical Property of anhydromesaconitine trifluoromethanesulfonate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of anhydromesaconitine trifluoromethanesulfonate

There total 1 articles about anhydromesaconitine trifluoromethanesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

mesaconitine (2752-64-9) + trifluoromethylsulfonic anhydride (358-23-6) → anhydromesaconitine trifluoromethanesulfonate (86817-64-3)

Guidance literature:

With pyridine;

DOI:10.1248/cpb.31.1422

Reference yield: 10.0%

anhydromesaconitine trifluoromethanesulfonate (86817-64-3) → C33H43NO9 (86817-65-4)

Guidance literature:

With N,N,N,N,N,N-hexamethylphosphoric triamide; In various solvent(s); for 3h; Ambient temperature; Irradiation;

DOI:10.1248/cpb.31.1422

Reference yield:

anhydromesaconitine trifluoromethanesulfonate (86817-64-3) → isodelphinine (1357-96-6)

Guidance literature:

Multi-step reaction with 2 steps

1: 10 percent / aq hexamethylphosphoric triamide / various solvent(s) / 3 h / Ambient temperature; Irradiation

2: 55 percent / hydrogen / platinum / ethanol

With N,N,N,N,N,N-hexamethylphosphoric triamide; hydrogen; platinum; In ethanol;

DOI:10.1248/cpb.31.1422

upstream raw materials:

mesaconitine

trifluoromethylsulfonic anhydride

Downstream raw materials:

C₃₃H₄₃NO₉

isodelphinine

Refernces