Technology Process of (2-(perfluorophenyl)ethene-1,1-diyl)dibenzene
There total 2 articles about (2-(perfluorophenyl)ethene-1,1-diyl)dibenzene which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
potassium fluoride; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; palladium diacetate; Trimethylacetic acid;
In
tetrahydrofuran;
at 20 ℃;
for 24h;
regioselective reaction;
Inert atmosphere;
DOI:10.1002/anie.201108211
- Guidance literature:
-
Multi-step reaction with 2 steps
1: potassium fluoride; bis(acetylacetonato)palladium(II); 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; propionic acid / 2 h / 20 °C / Inert atmosphere
2: potassium fluoride; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; palladium diacetate; Trimethylacetic acid / tetrahydrofuran / 24 h / 20 °C / Inert atmosphere
With
potassium fluoride; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; bis(acetylacetonato)palladium(II); palladium diacetate; propionic acid; Trimethylacetic acid;
In
tetrahydrofuran;
1: Oxidative Heck reaction / 2: Oxidative Heck reaction;
DOI:10.1002/anie.201108211
