Technology Process of C16H18IN5
There total 5 articles about C16H18IN5 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1: sodium hydride / tetrahydrofuran / 1 h / 20 °C
2: sodium hydrogencarbonate / water; 1,4-dioxane / 1 h / Reflux
3: ethanol / 1 h / Reflux
4: 8 h / 160 - 180 °C
With
sodium hydride; sodium hydrogencarbonate;
In
tetrahydrofuran; 1,4-dioxane; ethanol; water;
DOI:10.1021/jm4001314
- Guidance literature:
-
Multi-step reaction with 3 steps
1: sodium hydrogencarbonate / water; 1,4-dioxane / 1 h / Reflux
2: ethanol / 1 h / Reflux
3: 8 h / 160 - 180 °C
With
sodium hydrogencarbonate;
In
1,4-dioxane; ethanol; water;
DOI:10.1021/jm4001314
- Guidance literature:
-
Multi-step reaction with 5 steps
1: oxalyl dichloride / N,N-dimethyl-formamide; hexane / 1 h / 20 °C
2: sodium hydride / tetrahydrofuran / 1 h / 20 °C
3: sodium hydrogencarbonate / water; 1,4-dioxane / 1 h / Reflux
4: ethanol / 1 h / Reflux
5: 8 h / 160 - 180 °C
With
oxalyl dichloride; sodium hydride; sodium hydrogencarbonate;
In
tetrahydrofuran; 1,4-dioxane; ethanol; hexane; water; N,N-dimethyl-formamide;
DOI:10.1021/jm4001314