Technology Process of C24H24FN3O3S2
There total 10 articles about C24H24FN3O3S2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate / N,N-dimethyl-formamide / 20 °C
2.1: hydrogenchloride; water / tetrahydrofuran / 65 °C
3.1: sodium cyanoborohydride; acetic acid; N-ethyl-N,N-diisopropylamine / methanol; dichloromethane
4.1: water; sodium hydroxide / tetrahydrofuran
4.2: pH 6 / aq. phosphate buffer
With
hydrogenchloride; water; sodium cyanoborohydride; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; acetic acid; N-ethyl-N,N-diisopropylamine; sodium hydroxide;
In
tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2011.10.069
- Guidance literature:
-
C25H26FN3O3S2;
With
water; sodium hydroxide;
In
tetrahydrofuran;
With
hydrogenchloride;
pH=6;
aq. phosphate buffer;
DOI:10.1016/j.bmcl.2011.10.069
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: hydrogenchloride; water / tetrahydrofuran / 65 °C
2.1: sodium cyanoborohydride; acetic acid; N-ethyl-N,N-diisopropylamine / methanol; dichloromethane
3.1: water; sodium hydroxide / tetrahydrofuran
3.2: pH 6 / aq. phosphate buffer
With
hydrogenchloride; water; sodium cyanoborohydride; acetic acid; N-ethyl-N,N-diisopropylamine; sodium hydroxide;
In
tetrahydrofuran; methanol; dichloromethane;
DOI:10.1016/j.bmcl.2011.10.069