C₁₄H₁₁ClHgN₂O

Base Information

• Chemical Name: C₁₄H₁₁ClHgN₂O
• CAS No.: 1440513-12-1
• Molecular Formula: C₁₄H₁₁ClHgN₂O
• Molecular Weight: 459.297
• Mol file: 1440513-12-1.mol

Synonyms:

Chemical Property of C₁₄H₁₁ClHgN₂O

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₁₄H₁₁ClHgN₂O

There total 6 articles about C₁₄H₁₁ClHgN₂O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 44.0%

1-(2-oxazolinyl)-3-(2-pyridyl)benzene (1440513-11-0) + mercury(II) diacetate (1600-27-7) + lithium chloride → C14H11ClHgN2O (1440513-12-1)

Guidance literature:

1-(2-oxazolinyl)-3-(2-pyridyl)benzene; mercury(II) diacetate; In methanol; Reflux;

lithium chloride;

DOI:10.1016/j.inoche.2013.03.012

Reference yield:

meta-bromotoluene (591-17-3) → C14H11ClHgN2O (1440513-12-1)

Guidance literature:

Multi-step reaction with 6 steps

1: magnesium / tetrahydrofuran

2: potassium permanganate / tert-butyl alcohol

3: thionyl chloride

4: thionyl chloride

5: sodium hydride

6: methanol / Reflux

With potassium permanganate; thionyl chloride; sodium hydride; magnesium; In tetrahydrofuran; methanol; tert-butyl alcohol;

DOI:10.1016/j.inoche.2013.03.012

Reference yield:

2-bromo-pyridine (109-04-6) → C14H11ClHgN2O (1440513-12-1)

Guidance literature:

Multi-step reaction with 6 steps

1: magnesium / tetrahydrofuran

2: potassium permanganate / tert-butyl alcohol

3: thionyl chloride

4: thionyl chloride

5: sodium hydride

6: methanol / Reflux

With potassium permanganate; thionyl chloride; sodium hydride; magnesium; In tetrahydrofuran; methanol; tert-butyl alcohol;

DOI:10.1016/j.inoche.2013.03.012

upstream raw materials:

1-(2-oxazolinyl)-3-(2-pyridyl)benzene

mercury(II) diacetate

meta-bromotoluene

2-bromo-pyridine

Refernces