Technology Process of C26H29N7O3S
There total 8 articles about C26H29N7O3S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 7 steps
1.1: trichlorophosphate / acetonitrile / 1 h / 150 °C / Microwave irradiation
2.1: butan-1-ol / 3 h / 160 °C / Microwave irradiation
3.1: sodium hydrogencarbonate / water; dichloromethane
4.1: N,N-dimethyl-formamide / 4 h / 160 °C / Microwave irradiation
5.1: diammonium sulfide / N,N-dimethyl-formamide; methanol / 1 h / 100 °C / Microwave irradiation
5.2: 48 h / 23 °C / Microwave irradiation
6.1: ethanol / 1 h / 80 °C / Microwave irradiation
7.1: HATU; N-ethyl-N,N-diisopropylamine; ammonium hydroxide / dimethyl amine
With
diammonium sulfide; ammonium hydroxide; sodium hydrogencarbonate; N-ethyl-N,N-diisopropylamine; HATU; trichlorophosphate;
In
methanol; ethanol; dichloromethane; water; dimethyl amine; N,N-dimethyl-formamide; acetonitrile; butan-1-ol;
6.1: |Hantzsch Thiazole Synthesis;
DOI:10.1016/j.bmcl.2013.12.123
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: butan-1-ol / 3 h / 160 °C / Microwave irradiation
2.1: sodium hydrogencarbonate / water; dichloromethane
3.1: N,N-dimethyl-formamide / 4 h / 160 °C / Microwave irradiation
4.1: diammonium sulfide / N,N-dimethyl-formamide; methanol / 1 h / 100 °C / Microwave irradiation
4.2: 48 h / 23 °C / Microwave irradiation
5.1: ethanol / 1 h / 80 °C / Microwave irradiation
6.1: HATU; N-ethyl-N,N-diisopropylamine; ammonium hydroxide / dimethyl amine
With
diammonium sulfide; ammonium hydroxide; sodium hydrogencarbonate; N-ethyl-N,N-diisopropylamine; HATU;
In
methanol; ethanol; dichloromethane; water; dimethyl amine; N,N-dimethyl-formamide; butan-1-ol;
5.1: |Hantzsch Thiazole Synthesis;
DOI:10.1016/j.bmcl.2013.12.123
- Guidance literature:
-
Multi-step reaction with 2 steps
1: ethanol / 1 h / 80 °C / Microwave irradiation
2: HATU; N-ethyl-N,N-diisopropylamine; ammonium hydroxide / dimethyl amine
With
ammonium hydroxide; N-ethyl-N,N-diisopropylamine; HATU;
In
ethanol; dimethyl amine;
1: |Hantzsch Thiazole Synthesis;
DOI:10.1016/j.bmcl.2013.12.123