Technology Process of C31H42N2O2
There total 5 articles about C31H42N2O2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C23H38N2O3; phenylacetaldehyde;
In
methanol;
for 0.5h;
With
triethylamine;
In
methanol;
at 45 ℃;
for 16h;
DOI:10.1039/c3ob42309c
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: lithium aluminium tetrahydride / diethyl ether / 0.25 h / 0 - 33 °C / Inert atmosphere
2.1: sodium iodide / tetrahydrofuran / 0.42 h / 20 °C / Inert atmosphere
2.2: 1 h / 20 °C
3.1: methanol / 0.5 h
3.2: 16 h / 45 °C
With
lithium aluminium tetrahydride; sodium iodide;
In
tetrahydrofuran; methanol; diethyl ether;
DOI:10.1039/c3ob42309c
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: triethylamine / N,N-dimethyl-formamide / 16 h / 70 °C / Inert atmosphere
2.1: lithium aluminium tetrahydride / diethyl ether / 0.25 h / 0 - 33 °C / Inert atmosphere
3.1: sodium iodide / tetrahydrofuran / 0.42 h / 20 °C / Inert atmosphere
3.2: 1 h / 20 °C
4.1: methanol / 0.5 h
4.2: 16 h / 45 °C
With
lithium aluminium tetrahydride; triethylamine; sodium iodide;
In
tetrahydrofuran; methanol; diethyl ether; N,N-dimethyl-formamide;
DOI:10.1039/c3ob42309c