Technology Process of Disulfide, phenylmethyl 2-[[(phenylmethyl)sulfinyl]methyl]phenyl
There total 10 articles about Disulfide, phenylmethyl 2-[[(phenylmethyl)sulfinyl]methyl]phenyl which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid;
In
dichloromethane;
for 0.166667h;
Ambient temperature;
DOI:10.1021/ja00282a033
- Guidance literature:
-
Multi-step reaction with 7 steps
1: 90 percent / triethylamine / tetrahydrofuran / 2.5 h / Ambient temperature
2: 93 percent / lithium aluminum hydride / diethyl ether / 8 h / Ambient temperature
3: 91 percent / triethylamine / CH2Cl2 / 0.17 h / -10 °C
4: tetrahydrofuran / 0.5 h / Ambient temperature
5: 1.) silver nitrate; 2.) hydrogen sulfide / 1.) water, methanol, heating, 10 min; 2.) methylene chloride, 5 min
6: 97 percent / 1.) n-butyllithium / hexane; tetrahydrofuran / 0.5 h / Ambient temperature
7: 95 percent / 1.) 80 percent MCPBA; 2.) 5 percent sodium bicarbonate / CH2Cl2 / 0.17 h / Ambient temperature
With
lithium aluminium tetrahydride; n-butyllithium; hydrogen sulfide; sodium hydrogencarbonate; silver nitrate; triethylamine; 3-chloro-benzenecarboperoxoic acid;
In
tetrahydrofuran; diethyl ether; hexane; dichloromethane;
DOI:10.1021/ja00282a033
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 91 percent / triethylamine / CH2Cl2 / 0.17 h / -10 °C
2: tetrahydrofuran / 0.5 h / Ambient temperature
3: 1.) silver nitrate; 2.) hydrogen sulfide / 1.) water, methanol, heating, 10 min; 2.) methylene chloride, 5 min
4: 97 percent / 1.) n-butyllithium / hexane; tetrahydrofuran / 0.5 h / Ambient temperature
5: 95 percent / 1.) 80 percent MCPBA; 2.) 5 percent sodium bicarbonate / CH2Cl2 / 0.17 h / Ambient temperature
With
n-butyllithium; hydrogen sulfide; sodium hydrogencarbonate; silver nitrate; triethylamine; 3-chloro-benzenecarboperoxoic acid;
In
tetrahydrofuran; hexane; dichloromethane;
DOI:10.1021/ja00282a033