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Disulfide, phenylmethyl 2-[[(phenylmethyl)sulfinyl]methyl]phenyl

Base Information Edit
  • Chemical Name:Disulfide, phenylmethyl 2-[[(phenylmethyl)sulfinyl]methyl]phenyl
  • CAS No.:104324-63-2
  • Molecular Formula:C21H20OS3
  • Molecular Weight:384.587
  • Hs Code.:
  • Mol file:104324-63-2.mol
Disulfide, phenylmethyl 2-[[(phenylmethyl)sulfinyl]methyl]phenyl

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Chemical Property of Disulfide, phenylmethyl 2-[[(phenylmethyl)sulfinyl]methyl]phenyl Edit
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Technology Process of Disulfide, phenylmethyl 2-[[(phenylmethyl)sulfinyl]methyl]phenyl

There total 10 articles about Disulfide, phenylmethyl 2-[[(phenylmethyl)sulfinyl]methyl]phenyl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
With sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid; In dichloromethane; for 0.166667h; Ambient temperature;
DOI:10.1021/ja00282a033
Guidance literature:
Multi-step reaction with 7 steps
1: 90 percent / triethylamine / tetrahydrofuran / 2.5 h / Ambient temperature
2: 93 percent / lithium aluminum hydride / diethyl ether / 8 h / Ambient temperature
3: 91 percent / triethylamine / CH2Cl2 / 0.17 h / -10 °C
4: tetrahydrofuran / 0.5 h / Ambient temperature
5: 1.) silver nitrate; 2.) hydrogen sulfide / 1.) water, methanol, heating, 10 min; 2.) methylene chloride, 5 min
6: 97 percent / 1.) n-butyllithium / hexane; tetrahydrofuran / 0.5 h / Ambient temperature
7: 95 percent / 1.) 80 percent MCPBA; 2.) 5 percent sodium bicarbonate / CH2Cl2 / 0.17 h / Ambient temperature
With lithium aluminium tetrahydride; n-butyllithium; hydrogen sulfide; sodium hydrogencarbonate; silver nitrate; triethylamine; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; diethyl ether; hexane; dichloromethane;
DOI:10.1021/ja00282a033
Guidance literature:
Multi-step reaction with 5 steps
1: 91 percent / triethylamine / CH2Cl2 / 0.17 h / -10 °C
2: tetrahydrofuran / 0.5 h / Ambient temperature
3: 1.) silver nitrate; 2.) hydrogen sulfide / 1.) water, methanol, heating, 10 min; 2.) methylene chloride, 5 min
4: 97 percent / 1.) n-butyllithium / hexane; tetrahydrofuran / 0.5 h / Ambient temperature
5: 95 percent / 1.) 80 percent MCPBA; 2.) 5 percent sodium bicarbonate / CH2Cl2 / 0.17 h / Ambient temperature
With n-butyllithium; hydrogen sulfide; sodium hydrogencarbonate; silver nitrate; triethylamine; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; hexane; dichloromethane;
DOI:10.1021/ja00282a033
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