Technology Process of C16H23NO3
There total 6 articles about C16H23NO3 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
In
hexanes; isopropyl alcohol;
Resolution of racemate;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: trifluoroacetic acid / dichloromethane / 0.75 h / 0 - 20 °C
2: potassium carbonate / tetrahydrofuran; water / 0.5 h / 0 - 20 °C
3: hexanes; isopropyl alcohol / Resolution of racemate
With
potassium carbonate; trifluoroacetic acid;
In
tetrahydrofuran; hexanes; dichloromethane; water; isopropyl alcohol;
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: lithium diisopropyl amide / tetrahydrofuran / -78 - 20 °C
1.2: 0 °C
2.1: lithium triethylborohydride / tetrahydrofuran / 0.5 h / 20 °C
3.1: sodium hydride / N,N-dimethyl-formamide / 0 - 20 °C
3.2: 0 °C
4.1: trifluoroacetic acid / dichloromethane / 0.75 h / 0 - 20 °C
5.1: potassium carbonate / tetrahydrofuran; water / 0.5 h / 0 - 20 °C
6.1: hexanes; isopropyl alcohol / Resolution of racemate
With
sodium hydride; lithium triethylborohydride; potassium carbonate; trifluoroacetic acid; lithium diisopropyl amide;
In
tetrahydrofuran; hexanes; dichloromethane; water; N,N-dimethyl-formamide; isopropyl alcohol;
