triphenylantimony dicinnamate

Base Information

• Chemical Name: triphenylantimony dicinnamate
• CAS No.: 209287-24-1
• Molecular Formula: C₃₆H₂₉O₄Sb
• Molecular Weight: 647.374
• Mol file: 209287-24-1.mol

Synonyms:

Chemical Property of triphenylantimony dicinnamate

Chemical Property:

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Technology Process of triphenylantimony dicinnamate

There total 1 articles about triphenylantimony dicinnamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

triphenylantimony dichloride (594-31-0,34716-91-1,20265-29-6) + potassium 3-phenylacrylate (16089-48-8) → triphenylantimony dicinnamate (209287-24-1,71762-65-7)

Guidance literature:

In toluene; byproducts: KCl; sealed evacuated ampoule, 6 h, 100°C; filtrate concentrating and cooling;

Reference yield: 97.0%

triphenylantimony dicinnamate (209287-24-1,71762-65-7) + pentaphenylantimony (2170-05-0) → tetraphenylantimony cinnamate

Guidance literature:

In toluene; sealed evacuated ampoule, 100°C for 3 h; solvent removing, residue re-crystn. (benzene-isopropanol);

upstream raw materials:

triphenylantimony dichloride

potassium 3-phenylacrylate

Refernces