2-Propynoic acid, 3-[1-(phenylthio)cyclopropyl]-, methyl ester

Base Information Edit

Chemical Name:2-Propynoic acid, 3-[1-(phenylthio)cyclopropyl]-, methyl ester
CAS No.:104462-86-4
Molecular Formula:C13H12O2S
Molecular Weight:232.303
Hs Code.:
Mol file:104462-86-4.mol

Synonyms:

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Chemical Property of 2-Propynoic acid, 3-[1-(phenylthio)cyclopropyl]-, methyl ester Edit

Chemical Property:

Purity/Quality:

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MSDS Files:: SDS file from LookChem

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Technology Process of 2-Propynoic acid, 3-[1-(phenylthio)cyclopropyl]-, methyl ester

There total 4 articles about 2-Propynoic acid, 3-[1-(phenylthio)cyclopropyl]-, methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.5%

: 79-22-1
methyl chloroformate

: 104463-24-3
1-Ethinyl-1-(phenylthio)cyclopropan

: 104462-86-4
3-<1-(Phenylthio)cyclopropyl>-2-propinsaeure-methylester

Guidance literature:: With n-butyllithium; In hexane;

Reference yield:

: 83662-45-7
1-chloro-1-<(trimethylsilyl)ethynyl>cyclopropane

: 104462-86-4
3-<1-(Phenylthio)cyclopropyl>-2-propinsaeure-methylester

Guidance literature:: Multi-step reaction with 3 steps

1: 25 percent / 1.5 N n-BuLi / diethyl ether; hexane / 2 h / -78 °C

2: 78.5 percent / K₂CO₃ / methanol

3: 87.5 percent / 1.6 N n-BuLi / hexane

With n-butyllithium; potassium carbonate; In methanol; diethyl ether; hexane;

Reference yield:

: 104463-23-2
1-(phenylthio)-1-<(trimethylsilyl)ethynyl>cyclopropane

: 104462-86-4
3-<1-(Phenylthio)cyclopropyl>-2-propinsaeure-methylester

Guidance literature:: Multi-step reaction with 2 steps

1: 78.5 percent / K₂CO₃ / methanol

2: 87.5 percent / 1.6 N n-BuLi / hexane

With n-butyllithium; potassium carbonate; In methanol; hexane;