4-(2-nitro phenylthio)benzaldehyde

Base Information

• Chemical Name: 4-(2-nitro phenylthio)benzaldehyde
• CAS No.: 126585-08-8
• Molecular Formula: C₁₃H₉NO₃S
• Molecular Weight: 259.285
• Mol file: 126585-08-8.mol

Synonyms:

Chemical Property of 4-(2-nitro phenylthio)benzaldehyde

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 4-(2-nitro phenylthio)benzaldehyde

There total 3 articles about 4-(2-nitro phenylthio)benzaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-Chloronitrobenzene (88-73-3) → 4-(2-nitro phenylthio)benzaldehyde (126585-08-8)

Guidance literature:

Multi-step reaction with 2 steps

1: 89 percent / sodium ethylate / ethanol / 3 h / Ambient temperature

2: 1.) NBS, benzoyl-peroxide; 2.) silver nitrate / 1.) CCl₄, reflux, 15 h; 2.) acetone, water, room temp., 1 h

With N-Bromosuccinimide; Perbenzoic acid; sodium ethanolate; silver nitrate; In ethanol;

Reference yield:

para-thiocresol (106-45-6) → 4-(2-nitro phenylthio)benzaldehyde (126585-08-8)

Guidance literature:

Multi-step reaction with 2 steps

1: 89 percent / sodium ethylate / ethanol / 3 h / Ambient temperature

2: 1.) NBS, benzoyl-peroxide; 2.) silver nitrate / 1.) CCl₄, reflux, 15 h; 2.) acetone, water, room temp., 1 h

With N-Bromosuccinimide; Perbenzoic acid; sodium ethanolate; silver nitrate; In ethanol;

Reference yield:

2-(4-methylphenylsulfanyl)nitrobenzene (20912-17-8) → 4-(2-nitro phenylthio)benzaldehyde (126585-08-8) + 4-(2-nitro phenylthio)benzoic acid (126585-07-7)

Guidance literature:

With N-Bromosuccinimide; Perbenzoic acid; silver nitrate; Yield given. Multistep reaction. Yields of byproduct given; 1.) CCl₄, reflux, 15 h; 2.) acetone, water, room temp., 1 h;

upstream raw materials:

2-(4-methylphenylsulfanyl)nitrobenzene

2-Chloronitrobenzene

para-thiocresol

Downstream raw materials:

Acetic acid 4-[2-(2-diethylamino-acetylamino)-phenylsulfanyl]-benzyl ester

Acetic acid 4-[2-(4-chloro-benzoylamino)-phenylsulfanyl]-benzyl ester

Acetic acid 4-[2-(2-chloro-acetylamino)-phenylsulfanyl]-benzyl ester

4-(2-nitro phenylthio)benzylacetate

Refernces