1-phenyl-3,4-dimethyl-3-arsolene-1,2-bis(diphenylphosphino)ethane-tricarbonylmolybdenum

Base Information

• Chemical Name: 1-phenyl-3,4-dimethyl-3-arsolene-1,2-bis(diphenylphosphino)ethane-tricarbonylmolybdenum
• CAS No.: 160954-48-3
• Molecular Formula: C₄₁H₃₉AsMoO₃P₂
• Molecular Weight: 812.568
• Mol file: 160954-48-3.mol

Synonyms:

Chemical Property of 1-phenyl-3,4-dimethyl-3-arsolene-1,2-bis(diphenylphosphino)ethane-tricarbonylmolybdenum

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1-phenyl-3,4-dimethyl-3-arsolene-1,2-bis(diphenylphosphino)ethane-tricarbonylmolybdenum

There total 1 articles about 1-phenyl-3,4-dimethyl-3-arsolene-1,2-bis(diphenylphosphino)ethane-tricarbonylmolybdenum which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

Mo(CO)3(CH3CN)((C6H5)2P)2C2H4 (19349-53-2) + 1-phenyl-3,4-dimethyl-3-arsolene (73411-22-0) → 1-phenyl-3,4-dimethyl-3-arsolene-1,2-bis(diphenylphosphino)ethane-tricarbonylmolybdenum (160954-48-3)

Guidance literature:

In dichloromethane; soln. of metal-complex and arsolene in CH2Cl2 is allowed to stand at 20°C for 24 h (under inert gas); filtn. over Celite, concn. the volume, addn. of petroleum ether, filtn., recrystn. from CH2Cl2/Et2O, elem. anal.;

DOI:10.1016/0022-328X(94)88008-5

upstream raw materials:

Mo(CO)3(CH₃CN)((C₆H₅)2P)2C₂H₄

1-phenyl-3,4-dimethyl-3-arsolene

Refernces