Technology Process of C36H40N4O3S
There total 7 articles about C36H40N4O3S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 6 steps
1: dichloromethane / 20 °C
2: potassium hydroxide / methanol / Reflux
3: potassium carbonate / N,N-dimethyl-formamide / 45 °C
4: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium acetate / 1,4-dioxane / 85 °C
5: potassium carbonate; tetrakis(triphenylphosphine) palladium(0) / 1,2-dimethoxyethane; water / 85 °C
6: pyridine / 20 °C
With
pyridine; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; tetrakis(triphenylphosphine) palladium(0); potassium acetate; potassium carbonate; potassium hydroxide;
In
1,4-dioxane; methanol; 1,2-dimethoxyethane; dichloromethane; water; N,N-dimethyl-formamide;
4: |Suzuki-Miyaura Coupling / 5: |Suzuki Coupling;
DOI:10.1016/j.bmcl.2014.03.090
- Guidance literature:
-
Multi-step reaction with 7 steps
1.1: 1,1'-carbonyldiimidazole / tetrahydrofuran / 20 °C
1.2: 20 °C
2.1: dichloromethane / 20 °C
3.1: potassium hydroxide / methanol / Reflux
4.1: potassium carbonate / N,N-dimethyl-formamide / 45 °C
5.1: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium acetate / 1,4-dioxane / 85 °C
6.1: potassium carbonate; tetrakis(triphenylphosphine) palladium(0) / 1,2-dimethoxyethane; water / 85 °C
7.1: pyridine / 20 °C
With
pyridine; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; tetrakis(triphenylphosphine) palladium(0); potassium acetate; potassium carbonate; 1,1'-carbonyldiimidazole; potassium hydroxide;
In
tetrahydrofuran; 1,4-dioxane; methanol; 1,2-dimethoxyethane; dichloromethane; water; N,N-dimethyl-formamide;
5.1: |Suzuki-Miyaura Coupling / 6.1: |Suzuki Coupling;
DOI:10.1016/j.bmcl.2014.03.090
- Guidance literature:
-
Multi-step reaction with 5 steps
1: potassium hydroxide / methanol / Reflux
2: potassium carbonate / N,N-dimethyl-formamide / 45 °C
3: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium acetate / 1,4-dioxane / 85 °C
4: potassium carbonate; tetrakis(triphenylphosphine) palladium(0) / 1,2-dimethoxyethane; water / 85 °C
5: pyridine / 20 °C
With
pyridine; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; tetrakis(triphenylphosphine) palladium(0); potassium acetate; potassium carbonate; potassium hydroxide;
In
1,4-dioxane; methanol; 1,2-dimethoxyethane; water; N,N-dimethyl-formamide;
3: |Suzuki-Miyaura Coupling / 4: |Suzuki Coupling;
DOI:10.1016/j.bmcl.2014.03.090