Technology Process of C23H22N4O5
There total 11 articles about C23H22N4O5 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1: AcONa / Heating
2: phosphorus oxychloride / Heating
3: Heating
4: K2CO3 / dimethylformamide
With
potassium carbonate; trichlorophosphate;
sodium acetate;
In
N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2007.02.032
- Guidance literature:
-
Multi-step reaction with 5 steps
1: HBr / acetic acid / Heating
2: AcONa / Heating
3: phosphorus oxychloride / Heating
4: Heating
5: K2CO3 / dimethylformamide
With
hydrogen bromide; potassium carbonate; trichlorophosphate;
sodium acetate;
In
acetic acid; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2007.02.032
- Guidance literature:
-
Multi-step reaction with 10 steps
1: aq. NaOH / ethanol
2: SOCl2 / Heating
3: aq. NH3 / tetrahydrofuran
4: aq. NaOH / propan-2-ol / Heating
5: HBr / acetic acid / Heating
6: AcONa / Heating
7: phosphorus oxychloride / Heating
8: Heating
9: K2CO3 / dimethylformamide
With
ammonium hydroxide; sodium hydroxide; thionyl chloride; hydrogen bromide; potassium carbonate; trichlorophosphate;
sodium acetate;
In
tetrahydrofuran; ethanol; acetic acid; N,N-dimethyl-formamide; isopropyl alcohol;
DOI:10.1016/j.bmcl.2007.02.032