complex of N-formyl-o-aminophenol with triphenylphosphine oxide

Base Information

• Chemical Name: complex of N-formyl-o-aminophenol with triphenylphosphine oxide
• CAS No.: 79462-55-8
• Molecular Formula: C₇H₇NO₂*C₁₈H₁₅OP
• Molecular Weight: 415.428
• Mol file: 79462-55-8.mol

Synonyms:

Chemical Property of complex of N-formyl-o-aminophenol with triphenylphosphine oxide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of complex of N-formyl-o-aminophenol with triphenylphosphine oxide

There total 7 articles about complex of N-formyl-o-aminophenol with triphenylphosphine oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

Benzooxazol-2-yl-triphenyl-phosphonium; chloride (79462-53-6) → complex of N-formyl-o-aminophenol with triphenylphosphine oxide (79462-55-8)

Guidance literature:

With water; for 12h; Heating;

Reference yield:

triphenylphosphine (603-35-0) → complex of N-formyl-o-aminophenol with triphenylphosphine oxide (79462-55-8)

Guidance literature:

Multi-step reaction with 3 steps

1: 86 percent / 5 h / 170 - 175 °C

2: 90 percent / 20percent NaOH / H₂O

3: benzene / 4 h / Heating

With sodium hydroxide; In water; benzene;

Reference yield:

Benzothiazol-2-yl-triphenyl-phosphonium; chloride (79462-52-5) → complex of N-formyl-o-aminophenol with triphenylphosphine oxide (79462-55-8)

Guidance literature:

Multi-step reaction with 4 steps

1: acetonitrile / 8 h / Heating

2: 86 percent / 5 h / 170 - 175 °C

3: 90 percent / 20percent NaOH / H₂O

4: benzene / 4 h / Heating

With sodium hydroxide; In water; acetonitrile; benzene;

upstream raw materials:

Benzooxazol-2-yl-triphenyl-phosphonium; chloride

N-(2-hydroxyphenyl)formamide

Triphenylphosphine oxide

2-chloro-1,3-benzoxazole

Refernces