Technology Process of C36H47N7O4S2
There total 8 articles about C36H47N7O4S2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1: hydrazine
2: sodium cyanoborohydride; acetic acid / acetonitrile
3: sodium cyanoborohydride; toluene-4-sulfonic acid / tetrahydrofuran
With
sodium cyanoborohydride; toluene-4-sulfonic acid; acetic acid; hydrazine;
In
tetrahydrofuran; acetonitrile;
DOI:10.1016/j.bmcl.2013.12.058
- Guidance literature:
-
Multi-step reaction with 7 steps
1: N-ethyl-N,N-diisopropylamine; 1,1'-carbonyldiimidazole
2: sodium hydroxide; methanol
3: N-ethyl-N,N-diisopropylamine; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride
4: methanol; lithium borohydride / tetrahydrofuran
5: sulfur trioxide pyridine complex; triethylamine / dimethyl sulfoxide
6: sodium cyanoborohydride; acetic acid / acetonitrile
7: sodium cyanoborohydride; toluene-4-sulfonic acid / tetrahydrofuran
With
methanol; lithium borohydride; sulfur trioxide pyridine complex; sodium cyanoborohydride; benzotriazol-1-ol; toluene-4-sulfonic acid; acetic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; N-ethyl-N,N-diisopropylamine; 1,1'-carbonyldiimidazole; sodium hydroxide;
In
tetrahydrofuran; dimethyl sulfoxide; acetonitrile;
DOI:10.1016/j.bmcl.2013.12.058
- Guidance literature:
-
Multi-step reaction with 6 steps
1: sodium hydroxide; methanol
2: N-ethyl-N,N-diisopropylamine; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride
3: methanol; lithium borohydride / tetrahydrofuran
4: sulfur trioxide pyridine complex; triethylamine / dimethyl sulfoxide
5: sodium cyanoborohydride; acetic acid / acetonitrile
6: sodium cyanoborohydride; toluene-4-sulfonic acid / tetrahydrofuran
With
methanol; lithium borohydride; sulfur trioxide pyridine complex; sodium cyanoborohydride; benzotriazol-1-ol; toluene-4-sulfonic acid; acetic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; N-ethyl-N,N-diisopropylamine; sodium hydroxide;
In
tetrahydrofuran; dimethyl sulfoxide; acetonitrile;
DOI:10.1016/j.bmcl.2013.12.058