Di(3-methyl-2-nitrophenyl)-disulfid

Base Information

• Chemical Name: Di(3-methyl-2-nitrophenyl)-disulfid
• CAS No.: 60310-09-0
• Molecular Formula: C₁₄H₁₂N₂O₄S₂
• Molecular Weight: 336.392
• Mol file: 60310-09-0.mol

Synonyms:

Chemical Property of Di(3-methyl-2-nitrophenyl)-disulfid

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Di(3-methyl-2-nitrophenyl)-disulfid

There total 6 articles about Di(3-methyl-2-nitrophenyl)-disulfid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3-methyl-2-nitro-phenyl thiocyanate (60310-08-9) → Di(3-methyl-2-nitrophenyl)-disulfid (60310-09-0)

Guidance literature:

With sodium sulfide; In ethanol;

DOI:10.1002/hlca.19760590206

Reference yield:

3-methyl-2-nitrobenzoic acid (5437-38-7) → Di(3-methyl-2-nitrophenyl)-disulfid (60310-09-0)

Guidance literature:

Multi-step reaction with 5 steps

1: PCl₅

2: HCO₂NH₄

3: Br₂, aq. KOH

4: (i) NaNO₂, aq. H₂SO₄, (ii) /BRN= 3594799/, CoCl₂

5: Na₂S / ethanol

With sodium sulfide; potassium hydroxide; phosphorus pentachloride; bromine; ammonium formate; In ethanol;

DOI:10.1002/hlca.19760590206

Reference yield:

3-methyl-2-nitroaniline (601-87-6) → Di(3-methyl-2-nitrophenyl)-disulfid (60310-09-0)

Guidance literature:

Multi-step reaction with 2 steps

1: (i) NaNO₂, aq. H₂SO₄, (ii) /BRN= 3594799/, CoCl₂

2: Na₂S / ethanol

With sodium sulfide; In ethanol;

DOI:10.1002/hlca.19760590206

upstream raw materials:

3-methyl-2-nitro-phenyl thiocyanate

3-methyl-2-nitrobenzoic acid

3-methyl-2-nitroaniline

3-Methyl-2-nitrobenzenecarboxamide

Downstream raw materials:

2-nitro-toluene-3-sulfonyl chloride